Biomolecular NMR Facility

Department of Chemistry and Biochemistry

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NMR Services

  • Liquid NMR sample analysis.
    • Low concentration sample anaylsis capability
    • Batch sample analysis, and qNMR analysis
    • Expertise in small and biomolecule NMR analysis, structure elucidation
  • Consulting service on NMR methods, sample preparation, and isotope labeling methods
  • Workshops on NMR operation, 1D and 2D experiment setup, and data processing

Experiment Coverage (Please visit Applications webpage to see examples )

  • 1H, 13C, 15N, 19F, and 31P measurements. Broadband probe NMR measurements availabe soon!
  • 2D homonuclei and heteronuclei experiments, such as HSQC, HMBC, TOCSY, and NOESY
  • Wide experiment temperature range, 5-135 °C
  • Additional NMR experiments available upon request.

Sample Submission

Address:

University of Maryland, College Park
Biomolecular Sciences Building, Bldg# 296, room 1105
Paint Branch Drive
College Park, MD 20742
Attn: Daoning Zhang

Contact:

Dr. Daoning Zhang
Phone:(301)405-8239
Fax: (301)-314-0386
Email Contact

Sample Requirements

  • Sufficient sample amount is desired for reliable NMR analysis.
  • Liquid samples should have a minimum volume of 500 uL in deuterated solvents.
  • The facility provides common deuterated solvents for solid samples.

Data Processing and Delivery

  • Acquired NMR Data will be processed by the facility and sent to the customer electronically, including processed and raw data.
  • Frequent users may request a FTP (file transfer protocol) account for direct data access.
  • There is also a separate computer (Data Processing Station) in the NMR room for users to view and process NMR data.

Fee

 

Becoming an on-site NMR User?

A client with NMR operation experience can choose to run his/her own samples at the facility. Please visit our User Guide web-page for further details.